Extracting resin & chlorophyll separation | plant material
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- čas přidán 16. 02. 2019
- This process is inspired by BHO method
However in contrast we got resin material carried by ethanol.
Ethanol bottle didn't have concentration specified, so it may be reason why this happened.
There may be other methods to separate chlorophyll, But I was unable to find better one.
Maybe by controlling PH we could do this without using super volatile solvents like butane, but I haven't got more of a plant.. to experiment.
Music:
Spektr - Cypher
• Spektr - Cypher [Full ... - Věda a technologie
Beautiful video, beautiful English. Clear and straightforward 💪
Great choice of music! Also, wet your filter paper in advance with ethanol before charging it, you'll lose less product.
"Be careful of course, not like 5 year old"... love this video and advice.
If you are using propane or butane you might as well just blast it into bho
Well no shit Sherlock.
What if you want to extract CBD and chlorophyll and seperate.
Or just go ahead and become a crackhead
@@jamesshoemaker684 "weed bad I hate fun"
@@anthonyn1157 " cannabis good, chemicals bad." why do you hate fun?
An easy way to separate, you could doing mixed your ethanolic extract with two part of water and leave at 2-8ºC for 24 hours, the chlorophyll going to precipitateand you could take the supernatant and back to concentrate it, like the firt method used (inverse way to evaporated de hidroalcholic extrcat)
Hi. Can you go further on this method?
@Science Revolution Did u try?
I would really love to know how to do this. How would you seperate water from ethanol? Cold temperatures are defenetly not enough ^^
Like, seriously. Ethanol and water just mix with each other, how are you going to seperate them? I mean you could use salt, but you still end up with one salt water phase, and one ethanol phase which still carries both, the chloropyhl and the cannabinoids. So I call that BS
Skip the ethanol, it's a waste of time and money, wash your Bud directly in the butain....bob's your uncle.
never heard about propane being used as solvent. such a wonderful video
Freeze your bud and alcohol beforehand bro👌 then only wash it for 20 seconds at a time so you don’t get all the green oil from the chlorophyll and keep everything as cold as you possibly can. 🥶
It what I do and it comes out perfect every time, beautiful Amber color, people think they get more if they soak it for hours they just get more junk.
@@jbob3744 I do 5 minutes and get amber shatter but I use the 99.9% USP isopropyl and have everything at -40F the whole time. Then i make warm RSO as a second run and make dank edibles.
The quicker the wash, the better the final product, what about getting out fats and lipids?
@@HempearthTM maybe but possibly less thc probably better color and better looking with your method
How do I kno if all the isopropyl is gone I put the rso in oil it looks like tar it's gooey but I hears to get a lil bit and light it with fire and if it catches fire then it still has some but I think it's bull shit I hit it with my heat gun and it starts but I think I'm just burning it bubbling
Nice use of replacements for the lack of glassware. The working principle is the same, no matter how you improvise it.
Yeah that was a nice touch
You want to go cold. Freeze everything. If you freeze your bio mass and do all of this COLD..will be barely any chlorophyl present..less waxes, fats and lipids. Less filters needed..THANKS for sharing ur info
Activated charcoal cleans up the chlorophyll real nice. Use around 10% of the weight of your 'erb
This is awesome
Could you use a gel manicure UV curing machine to get rid of the chlorophyll?
UV was used only to see chlorophyll, is is not necessary to process
From uk southwales brilliant video and cheers very glad
For your own safety please never do any type of extraction with volatile solvents indoors. They may seem safe but the slightest spark and your life is changed forever. Just take the extra time to find a safe outdoor well ventilated area, and still take extreme precautions. Alcohol is simply better for full plant extracts which are meant to be consumed orally, not vaporized, so the chlorophyll is actually an added health benefit in such a case. However, for vaporizing alcohol extracts tend to contain some trace chlorophyll no matter what you do, so most people avoid it as a solvent for that purpose. Also be aware of the local/state/country laws. Always protect yourself both physically and legally. One love.
ok boomer
David Linnik ok tide pod
@@MrFragranceReview 😂 that was the best misused "ok boomer" response I've ever seen. Props. Lol
A simple way is you can set in in the sunshine and it will clear up the chlorophyl. what about using hot water with no special high-pressure apparatus, as oil floats on top of water principal? us a syringe or baster to extract the oil off the top and then reduce/evaporate the remaining water? what do you think?
UV rays degrade THC molecules
Dosent seem like lots of sunshine is available if homey has a sun box hahaha
Just freeze ethanol and do a quick wash extraction
@@Quickcat21MK ?
Do you have a procedure to extract resin
Good job comrade
you are a smart dude
You’ll get less chlorophyl with whole buds also dry them and freeze it.
Fantastic
You do have a really big UV source. Outside... Its always on...
Ve vill get Moose and Squirrel ....
Great vid
Do you have any references for this like scientific journals?
Nope
the video that you making sodium is very popular in "chinese youtube"in china,and,love your videos
YT algorithms are weird... thx for support :)
@@IlusysSystems oh no in china they have a seperate version of youtube where they reupload videos made on the real youtube to boost the popularity of their "Version" of youtube. Its seemingly unethical
@@ah4246 Ah I see... Well definitely unethical for some cases. My vids have CC license, so you can use this videos as you wish...
Hopefully I can spark some curiosity behind the great wall. This channel is my quest for freedom after all :)
Thank you boss
Why not start with butane extraction instead of using both.
Yes, someone gets it! Leave the clandestine lab work to the pro's
At school, we used acetone to dissolve chlorophyll.
Yeah, but you didn't use food grade/medical acetone. You don't want residual acetone in your body.
That circuit board table is dope
Thanks, you are first person that said this in 2 years :D
Wait what? this video has 100K views? wtf... Oh well.
@@IlusysSystems lmao that’s crazy thanks
@@IlusysSystemsBro, have you ever made oxytocin? I'm very curious about this. How is it extracted from the ergot fungus? I really want to extract it myself. Can you teach me?
@@IlusysSystemsBrother, no one on the entire Internet is making oxytocin! If you want to extract it and use it as a tutorial, the number of views will definitely exceed 100 million
@@user-in8bz3kd7d eeeeeeh I am not sure if you can make oxytocin from ergot fungus... I have just checked, and holly hell that is one complicated molecule. Cursed AF
Why not just cool the ethanol with dry ice instead of boiling it and avoid the chlorophyll problem almost entirely?
Didn't knew about such solution.
But even then, I don't have access to dry ice.
@@IlusysSystems Maybe you can order it on the internet? I find cooling alcohol in the freezer also works but I was thinking about chilling it in a dry ice and acetone/isopropyl bath. Should work wonders. You really don't need to add all that heat to strip the resin, alcohol will strip over 90% of the resin within the first few minutes. Also maybe the butane doesn't absorb the 'resins' because they aren't entirely non polar as they all have a hydroxyl group. When the butane hits the ethanol the temperature drops drastically and it will become more non polar so that may be why the goodies prefer to stay in the ethanol! It may be a little confusing because BHO is a very clear oil with very little chlorophyll, but thats only because the butane doesn't penetrate the cell walls to acces the chlorophyll. Very interesting procedures anyways I really enjoyed watching.
@@FOATE Thanks for info, my ethanol was at sub zero temperatures, which could explain, why chlorophyll wasn't dissolving.
@@IlusysSystems Yes exactly! temperature is a huge factor in the relative polarity of ethanol.
@@FOATE if you could help a struggling fool get better results I WILL listen.
I have access to massive amounts of low quality weed "leftovers". Trim, old bud, homegrown hang dried, recently picked colas and everything else not worth smokin..
I've made a very reliable BHO tube with shut off valves for each end that accommodate 8+ layers of coffee filter. Slowly filling the chamber with. Butane releasing pressure a few times to get more butane liquid in the weed material. (Assuming liquid butane + pressure=better yeald) 110 degrees Farenheit max purge followed by a week of sitting in a low dust/draft area. Room temperature
Dark with little high I thought the lack of oxygen was the high . I've learned to dissolve the "wax" in everclear for 2 days in freezer then separate with syringes... I get material on top and bottom of a clear everclear middle.
Should/could I use everclear differently by putting into the blasting chamber a couple tablespoons everclear just Before butane?. (Feel free to ridicule me if this all sounds moronic).
Do you have any suggestions other than buying "equipment".
I live in a retrofitted tiny home and have 12v power supply not 110. Super efficient freezer constant.
Other tha a 20ton press "dry sift" situation I dont have the time to operate. I'm at a loss as to what to do with all of this material...
I promise to gift an oz worth of grams to random folk if you can point me in the right direction...
Here's my email if it's easier louisep595@gmail.com...
Freeze flower for 48 hrs in chest freezer then take dry ice and and chill the ethanol mix the two together for 10 15 min . [time could vary) strain the hemp from ethanol and use a roto vap or hot water bath to get most of solvent out then purge it at 90f for a week. I would do a week if I can’t send a sample to a lab . I wouldn’t want anyone ingesting solvents
He doesn't have a separatory funnel, or a hot plate because he spent all his money on the roto vap.
Just use butane, it flash freezes the bud and strips it at same time...
A little activated charcoal in that filter would probably work
Retains a lot of THC, and also may contain heavy metals.
That was your only UV source???? Youu don't have the sun where you're at???
dat "resin" is some mary donchu wanna!!
Do an AC scrub to remove chlorophyll t hen filter through DC
hmm zajímavé :D
Nice equipment improv! But why not just start with a regular butane/propane blast? You'll leave all that chlorophyll behind on your first blast and you can still of course winterize the wax out of it afterwards with the ethanol if you want. Or is there a specific reason you went with this order of operations? Not claiming to be any kind of chemist here 😂
Not actual chemist either, I used propane ethanol mixture to decrease propane volatility, which kindof worked, but the result was not expected. So I shared... Also to get feedback for better methods
Sunlight works the best to get rid of greenish color.
It also renders much of the active compound THC inert
the sunlight or the chlorophyll will deactivate the thc?
Jay Tripoli THC degrades into CBN with sunlight uv.
For the ones saying thc gets degraded..have you ever made some and let it sit in sun. . I get tired of fools who read books or go off 2nd hand knowledge. A few hours in sunlight doesn't do a f ing thing..I am not a newbie to the cannabis game..made this shit 40plus times,have let some sit in the sun for weeks...I still got blasted on dab hits.
I'm betting that you could have just used a micron bag
When I make my bho I don't get that mine is caler shatter . I open blast . It's so good.
Forgo the reflux part, pack your Bud into a cylindrical object... reenforced pill bottle. Spray the butain through the cylinder, repeat a bunch... Same results without messing around...
Ethanol extracts the most THC and other compounds from the plant matter and it's much safer to collect again
Wash the finished product with distilled water or purified water you can rinse all the impurities out
Definitely not all impurities. In fact, for vast majority of plants, oily extracts are virtually insoluble in water
@@IlusysSystems have you ever tried the experiment if so you might know if not try
How you wash the producto dude?
@@IlusysSystems that’s because the oily extracts are the part you don’t want to extract when attempting to yield hash oil, particularly, in theory, a live resin type extract.
I’d rather smoke cannibidol oils than butane or propane impurities, even in trace amounts.
Nice...oregano...extract
Can I use ether instead of butane ?
Depends on plant I guess and what are you after. My goal was to find easiest way to remove chlorophyl, and probably least messy was suggested in comments - use activated charcoal
@@IlusysSystems I'm aiming to obtain an oil for eCig, with low amount of cloroplill and same level of thc and cbd
Looks dangerous a.f. w
"I can only think of one solvent that can do this. " names two
Don't use UV! Itbreaks down the good stuff for the plant ub question! Using Hexane should work.
Was tyts weed
What song was That, ripper??
Its Spektr - Cypher. It's work of art, really do recommend to check them out if you are into BM. Especially french...
@@IlusysSystems hey thanks for the reply. I really do like the song I'm gonna check out more.
Interesting. Dangerous but still interesting. Your doing a liquid liquid partitioning b/t ethanol (+ water?) And butane
yes (no water), but resin ended up in alcohol fraction which is weird..
@@IlusysSystems all the resin (cannabinoid portion) ended up in the butane?
@@Skunkhunt_42 No, it extracted into alcohol portion.
@@IlusysSystems ahh, I can't type. Did ya evap the butane fraction and see what was left behind?
@@Skunkhunt_42 yep it was mostly chlorophyll as I have tested by UV light. It's good question whether this was only extracted substance... TLC analysis would be good idea to do here, but I did not have any plates.. dunno maybe in future I would have to do this again, so I will look at this method more closely
gee whiz I wonder what type of plant matter that is
Well, any resinous leafy plant. This could be a sunflower. But it wasn't sunflower season that time...
Obviously it’s oregano 😭😭😭
What about super critical CO2 extraction?
Sure we can do that at home if we are crazy enough :)
Sure........ $100,000?
The Irony of you giving safety tips about butane while blasting inside next to a high watt lamp is just baffling 🙄 anyone reading this please don't copy this guy
Blasting?! 😂 this ain't dabs bud. His device was enclosed, similar to a lighter fill. This wasn't a tube onto a silicone mat
Z Polski jestes ?
Z cech ;)
@@IlusysSystems Blisko,
Pozdrawiam . 💪💪✌
Vacuum
That
More like borophyll!!!
Or is it a boat
Just use sunlight
Your filter papers were bleached you should use unbleached filter papers trust me
Best I got is a hair straightener and squeeze. Return to monke for me.
Fucking great video.
😐
ty for this video it was helpful also love how u stole footage from NurdRage hahahahaha
Damn, I just want some wax so i can dab some weed. I'll just use the flattenenin iron method..
UV destroy thc!
source?
@@IlusysSystems www.ncbi.nlm.nih.gov/pmc/articles/PMC2921171/ , should know that already , even if you destroy chlorophyll still a lot of tanines and other non wanted stuff on there, too much time on solvent too much processure an adding extra non sense solvent with some that could be done with frozen alcohol and 30 second wash to avoid all the steps you do.. with that system you finish with a low quality product
@@bundisensi From that papers it looks like degradation is not that dramatic. also type of UV was not specified..
Also I am quite happy to have resin with junk at this point - I really wanted to separate chlorophyll only.
But thx for info :)
@@IlusysSystems think what you want but dont fool people the type of UV is UV , los 10000 nm (4x10−7 m) y los 689075 nm (1,5x10−8 m..... THC on UV is the most efective degradation system , i guess think too smart and think nobody mind abaout that already , enjoy your concetrate with extrametacarpenes and destroyed thc molecules with extra celulose, but dont teach to poison people themselves
@@bundisensi nice english lol ...
Russians smoke weed? Coo.
I am not russian, and I don't smoke weed :D
But I am pretty sure, that russians do smoke weed :)
@@IlusysSystems Are you from Czech Republic ?
All this for a spliff🙄
go back to school
English mate....english would help.
spoiler alert: experiment failed. (!)
Technicky cistic? Gde to rob8s v cz??