Making Bismuth Trioxide From Elemental Bismuth - ElementalMaker
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- čas přidán 5. 04. 2021
- For an upcoming project I need Bismuth Trioxide, and here is the process I used to make it.
Follow the channel here: odysee.com/@ElementalMaker:8
Pure Elemental Bismuth Metal: amzn.to/3dxYyRg
In retrospect, I probably should have done a displacement with a hydroxide salt while the bismuth nitrate was still in solution, but the thermal decomposition in quartz glass was pretty neat to see.
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Thanks for watching! Please help keep the channel sponsor free by throwing a nickle in the hat at www.patreon.com/elementalmaker. Every patron gets a virtual hug and my unending appreciation. I will also build a rocket based shrine to worship you. One of these is a lie. Alternatively, saving this link as your amazon homepage can really help the channel out goo.gl/x1ehvA
Do you want the bismuth trioxide for crackling stars?
Where you located. I have a bunch of equipment you might be interested in.
Ok please no shrinet. Though.
Just keep on keeping on. Maybe a demo with some gallium?
Gallium and bismuth have a lot of interesting characteristics.
@@edwardarruda7215 Hi Edward, please email me at ElementCollector1001@gmail.com 👍
Little late to the party after a day in the shop but great vid! I saw you on NightHawkInLight's video about thermoacoustics and left a reply. Think you should do a video on thermoacoustics.
Ah, I see you finally remembered your youtube password
I think you needed to add some water, Red fuming nitric tends to stall out quickly. As there isn't any water to dissolve the metal salts they form a passivation layer stopping the nitric from reacting with more metal.
I'm a patron member now...it's been long awaited ....you can call me sugar daddy from now on and I'll just keep them washington's sprinkling down each month. Between you and Styropyro, Thought Emporium, Applied Science, Knight Hawk In Light, the old Cody's Labs, and the old Keystone Science, Great Scott, Mr. Teslonian, and Primitive Technology and King of Random, Nile Red/Blue, Nurd Rage, and sometimes Electro Boom, I am complete in my life from entertainment and useful knowledge. Thanks a million and I hope you make several millions because your a great creator. I can't get enough from you all.
Thank you so much Justin! Aka Mr sugar daddy 😂. I seriously appreciate your support my friend 👍
I'm honored just to be mentioned with those other creators. That means alot
king of random is a fuckin joke amongst those other creators lol
@@penguiin12 back when Grant was doing them it was pretty good. Along with some of the other creators. CZcams used to be way more awesome than it is now.
Damn! RFNA casually... jealous! Pleas use correct gloves though, nitrile will be destroyed in seconds and likely burst into flames. I do have plans on a RFNA video coming soon. Soon for me is a half decade 😅. Great video as always ;)
Note. Concentrated HNO3 Will auto combust Nitrile Gloves
Borosilicate and regular glass will pass uv a and b but almost completely blocks uv c.
please use vinyl gloves when working with nitric acid.
its the savest option thats cheap and available.
Yeah! Dude drop a little of that rfna on a latex glove! Caution! 🔥
Red Fuming Nitric, Holy Smokes Mate, just seeing that fuming on your video gave me rusty bullet hole Spasms. 🇬🇧🇺🇸👍.
Ok I am intrigued with the spectre of red fuming nitric... Please tell us more.
Working on that video now 👍
You are amazing man 🔥🔥
08:29 It's not tricky. Just insert your folded paper and rotate the paper by 180°. No shaking needed :-)
Hey now, ideas that good aren't allowed here 😁😁
oh man, reading this comment before watching that part made me feel pain
I made the same suggestion, not knowing you were 9 months faster than me. But in my defense, I'm not sure how I missed this video. I normally watch them all soon after upload.
If I had known that you needed bismuth trioxide I would have sent you a few ounces for this. We really need to get in touch. I'd love to use my hookups and my business to help support your channel with chemicals and elements. You could do sooooo much more with what I could supply you with.
you know, its really good then that you have the nitric acid now and not them cause its fuming.
Yeah it could have been quite dangerous to his family if it wasn't stored properly
Makes good crackle comp
Always enjoy 😉
When will you start making more rocket videos? I loved those!
After your comments, I really want to know what you are going to use the bismuth trioxide for.
Those nitrile gloves are not going to be doing you any favours, when using fuming nitric acid. In fact they are a positive liability, as they stand a good chance of bursting into flames if any of the acid touches them.
"I chemistry so hard NileRed laughs with envy" that had me cracking up :D
though you're setup might not be as fancy as NileRed's you still make great content and that i appreciate, Thank you! keep it coming :)
I'm jealous of your hotplate. I saw the video of you making it but some parts I can't get.
Wait, so the reason I haven't heard from you for a while is YT?
I'm subscribed and belled and still haven't had updates, and heard nothing about the last four vids.
Can you reiterate where would be a good place to follow what you do? Thx!
Not calling it "pepto bismol based oxygen" just to be on the safe side?
Glad to see you haven't blown your fingers off yet. It's been a bit since your last video and it's not just CZcams forgetting to notify me.
House projects have been taking up alot of my CZcams time unfortunately
@@ElementalMaker no problem. I haven't been able to upload much either because of family, work, and school. Then we have springtime coming up and yard projects...
Anyway, I need to check out LBRY so I can catch the other videos you put up in the meantime.
@@ElementalMaker house project=B channel content,,,,,
Do you want my leftover slag from making bismuth crystals? It has a head start in terms of making bismuth trioxide and won't matter if the oxide is all you want.
From memory when I made some of this trioxide I dissolved the bithmuth in nitric then somewhere along the line maybe after watering the solution down added sodium hydroxide which converted it all to the trioxide, it worked well in dragon eggs.
Nice! I probably should have gone the hydroxide displacement route, this thermal decomposition method was neat but not as simple and the wet method probably creates much better particle sizes
4:18 I read the round bottom flask measurement, I don't know if it's a glare or what but it looks as though it says "um!" I read it out loud as you said um yourself haha.
Can someone help me how to make potassium perchlorate at home
Should have added about 5mL of hydrogen peroxide to oxidize the NO2 back into nitric acid.
It you electric charge bismuth, does it create UV?
When is your next video? We want more! Anything at all!
What was the point of this trick and what percentage is red fuming Hno3? 90%?
Making some Dragon Eggs later with that Bismuth trioxide?
Quartz glass is great for taking fat dab hits too lol
I thought we did the stuff about conc HNO3 and latex gloves being a really bad idea? Seriously folks, don't do that. Better off getting it on your skin and washing it off immediately.
Red fuming nitric and gloves don't mix. This was azeotropic 70% concentration, so gloves are fine to use with it
9:00 you forgot the Chore Boy for your crack pipe.
Sorry , I'm having a hard time finding the "library" channel you said the next part of this video project would be posted. Something these days I'm quite interested in. Windstorm knocked down a very large willow limb, funny how things just fall into you lap :-) (Love the stuff on your channel) A link maybe?
It's now just called Odysee, so that might be why.
@@ElementalMaker Thanks, I'll keep looking. Darn youtube anyway!
Are you making dragons eggs with the bismuth trioxide?
For some reason Lbry and Odysee don't load for me (my computer is basically ancient at this point). Any plans to re-upload to Rumble or Bitchute?
Watch out what you mix that with ;-) If you mix such fine Bi203 with metallic fuels it can be quite ESD sensitive.
yay, another great vid!
Followed you on odysee can't wait to see what you do with it
Nice deal on the acid. I worked for a few years in an acid manufacturing plant, I was an instrument guy and had more than a few incidents you dont want your mother to hear about. My mum was a pharmacist, who retrained as an industrial chemist. looking foward to the video using the Trioxide is your LRBY name the same as youtube? 2x 👍
How the hell did I miss this video? 🤨
Its good :)
I tried odysee, but the videos buffer for about 3x longer than they actually play... I get 30 seconds of video then 1.5 mins of buffering, and it continues throughout the video that way. Am I doing something wrong or do they just suck that bad?
In occasion that seems to occur and I'm not sure why. Typically if I reload the page it fixes it. Usually they are pretty seamless.
@@ElementalMaker I had nothing but problems both times I tried it... I would delete CZcams in a heartbeat and send them the one finger salute if there was an actual competing platform, but with Google subsidizing CZcams's operational budget, i think it'll take gov't splitting them up as a monopoly.
What is this other plaftform for videos?
Ah right I should link it. Its a decentralized blockchain based video platform. Its the first real viable alternative to youtube I've seen, and I can post somewhat more energetic stuff on there without worrying about the YT bots gray listing my whole channel. Its called LBRY and Odysee (just a more youtube like frontend for the LBRY protocol)
@@ElementalMaker I'm going to need to check it out.
Nitrogen Dioxide.. "holy smokes!" 9:15 more like "unholy smokes!" 😉
Making dragon eggs I hope.. Maybe primers..
I've seen guys on the street in Kensington burning pipes with lighters just like you did in this video. I don't think they were making the same stuff as you though.
> I got about half a gram on the table in front of me
First time?
Was the yield A”bismuth”al?
This pun made me cough up blood.
My wife just loves a good dutch oven i mean i put the blanket over her head and she goes nuts flopping around and screaming.... lol we have fun! Great content look forward to looking you up on odysee
Ta-day..love it
Dude. Youre the best. Hilarious. Youre not bad at all. Fun shit man!
i wout really do this in a ice bath and let it get to ambient, also any tips on easy way to oxidize manganese?
For all the grey listing that youtube does the most fun chemistry I have learned I learned on youtube. Not saying you contributed to my corruption...but I'm not saying you didn't either. :)
I'd like to see you do something with tannerite how to make it and how to exploit it.
Are you going to make a crackle composition?
Do you have a link for where you bought the Bismuth?
Absolutely, there is a link in the video description 👍
Ozone smell for non chemist's is when you put a blanket outside on the sun ☀ and when you take it after some time it smells like ozone :) 😊
Everything that "smells like electricity", like a photocopier, this is actually ozone smell.
Why it happens?
(I'm referring to the blanket)
@@AccidentalScience uv light splits oxygen into o o and than because they are radical they quickly make O3 and blanket fibers trap ir
@@emmepombar3328 I would not agree, it's a very specific smell
@@unity4alle1 ok, thank you. Frankly I do not recall to have ever felt the smell of ozone from blankets put on the sun, I'll try to pay more attention next time to check it out. Cheers.
10:36 Your yield is A-Bismul? 😁
This comment made my night 🤣
@@ElementalMaker
My work here is done. Now I must... AWAAAAAAY!
Would love to see you do a video on Nitric Oxide production by high voltage electrical discharges. For fun you could do a conversion to Nitric Dioxide after. I imagine you would have a more creative way of doing so.
I've been wanting to do a birkland eye reactor for a long time. I just need a neon sign transformer.
@@ElementalMaker $40 online for 10Kv on amazon. Cheaper on ebay ($20). Looking forward to this couldn't you use an old microwave transformer and just redo the windings. Some maths and chemistry in one video as a plus of recycling a transformer.
Hope it's not red fuming,it's red fuming :)
Fuming red nitric acid. Ok. Some of the scariest chemical. An old assayed once used it to show me some weird stuff. He had been a college chemistry professor many years before. His demo included what just the fumes would do to steel and copper sheets.
If you find a strange flower by the name of Audrey
Growing over your dry-well don't feed it!
What do you use bismuth trioxide for?
Crackling stars
Whoop I stopped what I was doing to watch this
Yay chemistry
Nile red laughs with envy... but Nile BLUE... is fuming! 🤓😜
Would HCL have any effect on bismuth?
Is there way to get sulfur out of molasses?
It feels dangerous just watching it! 😂
What are you going to do with Bi2O3...?
Dragon's egg? 😄
But of course, he is. :)
An enthusiastic "TODAY!" intro! Funny that you procured that conc. hydrogen nitrate from the Estate of a deceased chemistry hobbyist. Lucky you! Where I live (England, which is still a Nanny State even though we have left the EU) such a chemical procurement would be forbidden on 'Elf and Safety'.
can you say what you're making with the trioxide in the comments?
I am a little confused. You ask to support on patreon so you don't have to worry about the CZcams demonetization, but then you are actually going to do the experiment somewhere other than CZcams anyways. I understand wanting to not be under their thumb, but I will say that at least for myself, I won't follow away from CZcams as it has apps on all my devices including my tv, and it is rare that I watch videos sitting at my computer. That is just my two cents and I enjoy your content and would really enjoy seeing the energetics you have planned, but only if I don't have to follow you elsewhere to see them. Hopefully this doesn't come off as too negative but more enlightening to what at least some of your audience is likely to do if you ditch CZcams for a less convenient platform. Have a good one!
Energetics won't just get you demonetized on CZcams, they'll get your channel completely terminated. Not something I'm willing to risk. I wish it were different but youtube ain't what it used to be
@@ElementalMaker Fair enough. Maybe make a second channel on CZcams for that and then if it gets removed you haven't lost everything.
@@chris993361 You mean a second ban evasion account that is against the ToS?
@@donpalmera I fail to see what that matters, as they arbitrarily decide when something is or isn't against the terms of service anyway. But it doesn't have to strictly be that anyway. This is his building or vlog channel and the other one can be his energetics channel. Different content making it not a ban evasion account.
@@chris993361
If you create a throwaway account because you think it might get banned that is ban evasion. I'm not saying what youtube does is right or wrong but people have tried the multiple channel thing and even used channels registered to other people in the past. They got caught and lost all of their channels.
What a pain in the ash 39 min and I think I have signed over my first Born and still have not seen what I was looking for what a odisy
Link is in the description, it'll take you right to my channel. It's very user friendly and similar to CZcams
My man 👍 be careful with stuff
Can some one explain to a non chemist why the red fuming is so bad and what other kind would you rarther it be?
Red fuming is a lot more concentrated and thus much more dangerous, it will quickly set many things on fire if it contacts them including your safety gloves
So flame-retardant treatments or optical glass?
In my drug using days i learned that if u have a scoop of powder or crystals, if you stick the whole scoop in or the whole fold of the scoop and hold the tube level and just rotate the entire thing then you wont spill any and get the most inside the quickest... lol. Ohh the jitters ensue... drugs are bad mmkay..
I feel like you are a few different ppl.....like the Reses Candy narrator......
10:36 would you say your yield was "abismuthal"?
Tryna make crackling microstars?
There should be a crackhead trigger warning at the start of this video 😂😂
Sounds like your going to make dragon eggs or crackle
Thought I was on NileRed for a second
Why not react the Bismuth with nitric and then mix it with bicarb? The insoluble Carbonate just thermally decomposes to remove carbon dioxide and what’s left in the solution is sodium nitrate with a bicarb impurity.
Primers on a hot plate.. Way to go...
"Despite having half a gram laying in front of me.." Man you missed it.. A couple weeks ago I had four sessions where I had 100+ grams laying in front of me. Though that was weed not bismuth trioxide lol. We ended up with ~436 grams out of 4 plants, unfortunately one or two plants went hermaphrodite on us and produced seeds in everything so it's mostly shit looking and requires a LOT of work removing all the seeds before use. Oh and before anyone freaks out, I live in California, recreational use/home growing is legal and we have all the filters and whatnot. And if anyone wants to know what we grew, 2 were a hybrid called Dragon Fruit (which had absolutely no fruity smell at all even though it was supposed to smell just like the fruit) 1 was Panama Pupil V3 I believe and another was Mexican Bacon.. both those are sativas... much taller plants close to the same yield. Both DF plants produced 4oz (well one was 4.1) and the two sativas were in the high 3's.
Uh, alright then...
Ok but any concentrated nitric reacts with metal to produce NO2 fumes, no? Should have poured it out by itself to see if it was actually RFNA…
And the yield is... abysmal ... You missed the chance, you could have said a pepto Bismol.
Edit: Chemical jokes get no reaction :p
Yield actually wasn't bad if you paid attention
@@ElementalMaker I know my bad jokes stink even more than any mercaptan could ever dream of :p
Interesting stuff by the way. Having studied chemistry myself I'm quite impressed, by both the work put in the realisation of your videos, and the way you manage to make it lively and understandable. Congrats.
Do you think you might be demonized for a few innocent dragon eggs which you supposedly made this s#it for
Seems possible though
... sadly
5:54 total missed opportunity for a bad pun. "We should be in bismuth" instead of business
Would you say your yield was peptobysmal? Lol sorry.
I also own some suspiciously yellowed box fans. What amateur chemist doesn't?
That's like $80 in primers... LOL
Sooooo.. is it known how the pervious owner of that RFNA passed? It's a damn shame either way. Just be careful with that juice.
Not a clue but opefully it was peaceful and pain free.
Put the next video on (1/8 byte) - Chute. Sorry, the original name leads to an auto deletion of the comment!
I really hate the CZcams censorship.
6:14 still not on the lvl of the poormans chemist