Making Nitrotetrazole
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- čas přidán 31. 01. 2020
- We need some of the energetic compound 5-nitrotetrazole, so we make it. What could possibly go wrong?! (Warning: contains a few moments of high panic)
Thanks to ReactiveChem for a good video reference on this: / @reactivechem7408
The patent I am following: patents.google.com/patent/US9...
Subreddit: / explosionsandfire
Twitter: / explosions_fire
Patreon: / explosionsandfire
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Music: from Aphex Twin's soundcloud dump, track name: Pretend Analog Extmix 2b - Věda a technologie
You're telling me chemical supply company didn't want to be associated with garden shed based energetics research shocking
Interesting video as always thanks
Ah I forgot to insert the "THEN FILTER, WASH WITH A LITTLE ICE COLD WATER AND DRY THOROUGHLY ON THE PUMP", you'll just have to imagine it
RIP Chem Player,
Gone but not forgotten.
P U M P
You chemists made me want to get lots of glass just to make stuff from my greenhouse lolol
But what if my imagination is shit? Thats why i youtube!
@@Rhodanide theres a reupload channel.... But no new stuff. I actually downloaded all the Chemplayer Reupload videos incase that gets deleted too.
Yes, this is just about the perfect amount of questionable shed chemistry that I need in my life right now.
Ta mate.
+
Your equipment is beautifully ghetto
mattroski007 That’s a bit reductive. A poor craftsmen blames his tools. A master craftsmen is as good as his best tools.
That is to say, if you’ve no skill it doesn’t matter what tools you have. But if you have the skills, your upper limits are based on having the right tools, at the right time. And quality and precision, are factors that make certain tools the right tools.
Obviously for his use, these tool need not be of the highest quality.
chickenmonger123 I believe that matt’s point was that even though he doesn’t have the best equipment he has the brains to figure out how to use what he has to its fullest, and probably beyond what it was mean to be used for. Which rather than being reductive is a massive compliment.
i subscribed as soon as i saw the broken test tube being used to pour acid, we need to start a gofundme to get nilered to send him some better glass!!
Looks Like a method Lab LoL
Like a Meth lab
I love the combination of an aussie bloke in his shed and compounds of questionable liability :D -Cheers from Amsterdam :)
Questionable "liability," or "lability?"
@@techobsessed1 gotta be both to be a good chemist.
Sounds like something I should be doing...
@Coma White Or fungi of questionable legality
I like compounds of questionable liability from Amsterdam
always fun when all your chemicals are expired
Yeah I am very slow to do things, and I sometimes really get punished for it
@@enragedlemon3115 some do. Some are unstable enough to react with oxygen and/or sunlight if you leave then to long
@@enragedlemon3115 it can depend on the chemical. Over time they can evaporate and other such changes like oxidizing, but generally once you keep them sealed in appropriate conditions you should be good. Just check before you use them.
@@nobody-pr7fg A big exception is ethers, which can form highly explosive peroxides. Never use expired ethers. My professor once told me a story of a researcher who tried to open an old container of ether and blew away his stomach.
@@Twewy13 good to know
Your defeatist attitude as to how much tetrazole you could possibly ever use in energetics disappoints me gravely.
You're right, perhaps it is a 'should ever use' not 'could ever'...
High-level energetic chemistry in a rusty shed.
You are my spirit animal.
"Woah! Ah, it did the thing! Holy shit, look at that" me to my PI when I finally get good data mate.
Yeah bloody oath, I feel that
I like to imagine that there is a place where everyone uses a Private Investigator for stuff, and you both live there.
Yellow chemistry is bad chemistry
Chlorine for me is the worst. Accidentally left my windows open while I was outside doing some HCl chemistry and rusted a bunch of stuff
@@masondaub9201 chlorine is green
M'kay
But, like all good chemistry, liquid chlorine is yellow-amber.
@@ExtractionsAndIre I more meant haven't had any bad things happen with yellow chemicals yet
9:37 "I have quite a bit of Nitric Acid. That's not a flex, it's just a point." I laughed a little harder than I should have, there.
Good stuff.
It’s always a happy day when I see a notification that you’ve uploaded on either of your channels. Your stuff is seriously my favorite on CZcams
Thanks mate!
something you never wanna hear your chem teacher say, "woah I did the thing! Sick!"
Hopefully your chem teacher is also not teaching explosives synthesis from their shed
I love how not oxygen sensitive your chemistry is, it really makes me weep for the procedures I have to follow
Often I think about doing some air sensitive chemistry, like getting an argon cylinder, setting up some sort of glove box... but then I think about how unforgiving most of it is, and how I probably couldn't pull it off
@@ExtractionsAndIre Ever thought about finding a compound to use as an inert liquid seal? Something nonreactive but less dense than the product that's oxygen sensitive, so a layer of it could float on the reaction vessel... I'm probably talking about unicorn piss, but hey, it's not yellow.
@@ExtractionsAndIre now that I would love to see. The ghetto glove box made entirely from what you can get at the hardware store! What about for your 33.5k subscriber special????? 👀👀
I think this is the most ghetto chemistry channel I've ever watched and I love it so far
If the company didn't want you to name them, I was 100% sure they weren't sponsoring the video.
I mean honestly, I asked and I never saw a reply, so I just assumed
Probably a fair assumption.
I'm sure they simply couldn't come up with a polite enough way to say "LOL, no fucking way bro, but thanks for asking". :)
@@ExtractionsAndIre Yep. Better safe than sorry.
sixstringedthing We would highly appreciate that you do not disclose any information about our company. However, we are appreciative of your question.
"I have a lot of nitric acid!" Whoa okay, stay chill there. o_o
When the solution started bubbling and temp inc, i was like oh shit. The think calming thoughts didn't help. It feels like you're always 5cm away from death somehow.
It was a little scary! And avoidable, if I'd been better!
@@ExtractionsAndIre also is it not possible to do nitration after removing nh2by diazodization and then H2po2 to remove the diazonium salt? You've got soany nitrogens i think just dilute hno3 would do it on the ring.
Or does it explode somewhwre
@@ExtractionsAndIre also I'm no chemist, I'm just a highschool student remembering all the organic reactions for marks
Not exactly sure but you can't nitrate it directly, the ring is pretty weird and doesn't behave how a benzene group would
Yeah, this is Australia. We are ways 5cm away from a deadly animal
When you're in a community where saying you have quite a bit of nitric acid can be seen as flexing...
I love that you show your errors. It's both fun to watch, and demonstrates important points about how things CAN turn out, and how to identify and address problems.
Can't help but notice the Melbourne Bitters in the background
All your content is so very entertaining, your chaotic energy paired with toxic and energetic compounds is the perfect combo! I get so pumped whenever I see you've posted
Ahhh a run away reaction, god that's infuriating and scary when that happens.
I think more Chemists should use random profanity in their explanations.
I feel so early, hasn’t been demonetized yet!
That channel name change is big money, btw don't forget to buy gloves
I really like milk
Milklover 425 me too
OMG you two are like fuckin twins!
I really like war.
Big fan of milk. Used to be able to drink 2 L of chocolate milk in a few hours and be fine, but these days my body is weak and I shit myself by the 7th glass :(
@@ExtractionsAndIre , only 1 cup for me.
always looking forward to new vids! really glad to see you're back at your old antics of seeing how many nitrogens you can squeeze into a single compound.
As always, outstanding music choice. Thank you.
Love the videos, using these as a way to gauge my own chemist hobby while I'm in Uni. Great learning experience.
Always enjoy watching ya work, be safe and ty for every video =D
Thanks for watching!
Bloody fascinating stuff, mate. Keep up the good work.
Love your videos! Keep it up can't wait for the next one.
2:30 I love the broken glassware😂😂😂
Again your level of awesomeness can not be surpassed love this channel
I really love this channel.
Keep the booms coming.
"But I have a solution" proceeds to show powder, not solution.
Love the channel love the banter young chemist out here with the content
You are so smart. I love they way you make this entertaining while showing your huge, broad knowledge of chemistry.
Another excellent video! Thank you!
You have managed to reignite my interest in chemistry
That's great to hear, glad you like the videos!
Hey i'm liking the use of "that chemical supplier" , one of my favourite suppliers!
Gods damn I love your work!
good to know you are not dead from the fires
It's always nice to not be dead. Lab didn't burn down either!
You should do a video on perchloric acid and some cool reactions with it, btw love your vids. Keep up the the good work 👍
* - What are you doing as a hobby?
E&F -I like to do a bit of chemistry.
* -Oh that's so cool! Are you making your own soap or something in those lines?
E&F -I tame the fire demons...
* -...
* -cool
Hey I had that video where I used soap! Granted, I'm going to turn it into napalm, but it was still soap chemistry for a brief moment
@@ExtractionsAndIre Yeah if I remember correctly the solution kept solidifing.
Btw. How likely it is that you will post some more extraction videos in the near future(Q1-2)?
Just wanted to say I'm glad you made a new channel and are still uploading:)
Great video as always. I wish I had my own land away from people so that I could play more in depth in energetic chemistry, but unfortunately I live in an apartment town-home community. I usually just play with minerals now and extract whatever comes out of them with acids & bases. So, I have tons of unknowns along with more arsenic and thallium than I know what to do with, and yet, I still bought extremely pure arsenic and thallium online for my periodic table collection.
bless ya for this sick content!
I did the same thing the first time I did this synthesis lol.
Great job!
Finally another video!!
Rewatching for the 4th time, and noticing the repurposed codeine cough syrup bottle. Gotta love it
never change your taste in music!
"It did the thing" is literally me in every reaction
"That's not a flex, it's just a point." hahaha. I don't even understand half the stuff you talk about, but it is always interesting watching in the end. Keep up the good stuff amigo
5:40 goddamn it that's why I'm here!
Bought an old corning stirrer hotplate on ebay a while ago for making PCBs. The stirring control was broken though and stuck at full speed. After resoldering both the power board and control board twice I finally tracked down the issue after basically reverse engineering half the control circuitry. Turns out there was one broken trace coming from the ir "rotary encoder" (used the fan blades on the motor for feedback) near a pin it passed through. Totally worth the effort for the price though
Fantastic videos made!
Archimedes; "Eureka."
Extractions&Ire; Woow, it did the thing, holy shit, look at that, that's fucking sick as!"
Giving me Nurdrage, Cody's Lab, NileRed vibes all at once. Glad I found this video, I'll be watching a lot more of yours in the future :)
my boss, an idiot - MSDS sheet, label and safe storage containers
Mega brain genius - Milk jug labeled "cobalt waste"
Such a Flex with the nitricacid
Oh shit that's right, I need gloves. Thanks bro.
We've got this, go team
@@ExtractionsAndIre Got it done, and it only took two hours of going full ADD on various projects to come back here and be again reminded. So...
_Fackin nailed it!_
Excelent My brother.
"Rapid update, its out of control"
yeeesssss aphex twin
Sick as what
4:30 "Thats fking sick as"
Southern aussie showing
The fact that you screwed up is probably what saved your skin on the overheat.
It was self heating like crazy, it doesn't do that if you do it correctly!
That was beautiful
"I have quite a bit of nitric acid. ...
That's not a flex. It's just a point."
I'm looking forward to the start of next month's video,
"I forgot to buy more gloves"
Every video for the next 6 months
3:30 AHHHH It's *Y E L L O W*
Lol sounds like you'd love new Mexico states proportion lab .... It's always great watching you don't beat around the bush and are quite blunt unlike the rest of the community thanks
Nice synth, I feel the pain with the sodium sulfate. I always evaporate all the water and use acetone to extract the sodium nitrotetrazole (it leaves everything else behind)
Oh yeah acetone, that's a great idea! I did actually use your video as a good reference for this btw, I'll link your channel in the description
Extractions&Ire wow, thanks. I hope you plan on making another nitrotetrazole vid because I loved ur first one.
Yeah there'll be at least 1 new one, on new complexes!
Not a chemist BUT I NEED TO KNOW WHAT THAT THING IS THAT TURNS INSIDE A FLASK TO STIR I NEED MORE OF THAT IN MY LIFE
Ahmet Fatih Usta It’s a Teflon covered bar magnet, aka; stir bar. It’s rotated by a more powerful magnet that spins under the hot plate. (In case you see this comment)
Chaos reigns supreme. Again.
Please keep up the videos. I fucking love your videos. You 1) have a damn good sense of humor and 2) a really great mind for showing the rest of us just how beautifully terrifying our natural world really is. The sights sounds and surprises that are there in everything around us. But enough kissing ass. Keep up the channel please. But change nothing unless you can upgrade things you'd like to. I'd love to support your work a bit with what I can.
A partial runaway nitration is an insane method. Is it one of the easiest ways? Yes, it sure is. Is it the safest method? No, no it is not. Methods lile this are what tricks amateur energetic enthusiasts into thinking it is a simple undertaking, but that is actually a very advanced method and must be monitored very closely. Cool video either way though.
That broken grad cylinder is triggering me
It still works!! ...slightly
lol i saw that too and laughed.
of course he'd be using a broken grad cylinder. wouldn't be E&F without aussie accented swearing and delightfully ghetto equipment.
Part of me wants to see what you can do with a proper lab. But we cannot abandon the shed, it’s part of the charm.
Anyways the only thing I really care about is him having access to a top of the line fume hood.
Installed in the shed.
Oh and a wind screen lol
Ngl I like watching these vids so I can say fancy words and sound smart to myself
YES!
Another great video!
Thanks!
@@ExtractionsAndIre Out of curiosity:
Over the years, some of your videos have been removed from this particular location.
Is there any one source, where I could find all videos from all your previous channels?
From the main channel, you can see the old videos here! www.bitchute.com/channel/explosionsandfire
@@ExtractionsAndIre Thanks dude!
My collection was missing a few of the older ones.
went to the sci channel and told the guy who said this stuff goes off when look at it funny,
" tom made some, on extractions and ire, in a shed, with a box of scraps"
Dude Clean.
can be used in blasting caps and considered for small arms primers in a compound (secrete compound as most patents for making this is pretty old -1970's) as the salts, copper, are pretty non reactive with copper brass .. primary initiators are pretty violent, so do not make without the right legal requirements adhered to .. [yes, that came up in my search]
That molex connector lmao!
sounds so whip! you could be a cowboy or a chemist.
I would love to see if chlorine trifluoride really sets titanium and concrete on fire, if you could try that one that'd be the shit dank hill out.
Ambien makes me apaet of your expermiements, let me no what to send energy too
This bad boy contains so much Aminoguanidine Bicarbonate!
*slaps roof of bottle*
Since from the research paper, Free Nitrotetrazole compound is quiet sensitive due to impact and friction. so is there a way to make NH4CuNT from Sodium Nitrotetrazolate NaNT? Or make NH4CuNT more directly without Free Nitrotetrazole exist as an intermediate?
That’s a big ass beaker of boom shukalukka
"That's not a flex that's just a point"
Just that sad, sad, broken graduated cylinder. XD
If you haven't done so already, please make a video on Cold Detonation Physics, like dry ice and powdered Mg.
It's like Röyksopp meets Young Einstein to put bubbles in beer. Hey Mate?... But the stuff this guy plays with will kill ya faster than a King Brown...
That looks like a very unstable molecule. Full of unhappy nitrogens.
I would love seeing you on cold ones podcast
4:20 What's that, working w/ pure reactants really makes a difference?
What are you using as a coolant in condenser? Dyed water or some PC/ car coolant?
It's just green water! It's green because green