Recrystallization and Melting Point Analysis

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  • čas přidán 28. 08. 2024
  • Now that we have covered some important separation techniques, let's take a look at a purification technique. Sometimes a chemical reaction will produce a solid, which can precipitate from solution. But these crystals typically contain impurities from solution that were trapped in the lattice as it formed. After we isolate these crystals, we can purify them via recrystallization. This is where we dissolve them in a particular hot solvent that will then retain any impurities before cooling it down such that it can crystallize again. We will also learn how to assess the purity of our recrystallized product using melting point analysis. This is neat stuff!
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Komentáře • 55

  • @nathanmermilliod3135
    @nathanmermilliod3135 Před rokem +27

    Perfect video and explanation of concepts, and just in time for my students’ lab practical on recrystallization. Thanks Professor Dave!

    • @23100Battlefield
      @23100Battlefield Před rokem

      I had my lab on this three weeks ago! Wish Dave had this video earlier, you really have labs late in the term, it's our exam period rn

  • @thomaseddyson362
    @thomaseddyson362 Před rokem +9

    Thank you. I always appreciate the effort you go to with your videos. Well presented with just enough of the required ephemera.

  • @cancan1231ify
    @cancan1231ify Před rokem +4

    Hey, I have friends and roommates that work for Thermo Fischer scientific. What a fun coincidence that they sponsored one of my favorite CZcamsrs.

  • @eddielikesfish7114
    @eddielikesfish7114 Před rokem +6

    i literally just learnt about this in chemistry lol. we are going to be making asprin with this method in january

  • @henna_nenna
    @henna_nenna Před 7 měsíci +1

    you are saving the life of every ochem college student thank you so much

  • @harrybrielmann189
    @harrybrielmann189 Před rokem +1

    very complete! And I agree that trituration (forcing the solvent out by the addition of a less soluble solvent) often results in a less pure product.

  • @hananehanane3860
    @hananehanane3860 Před rokem +6

    I hope to see more techniques explanation in your channel. Thanks Prof Dave

  • @louisnemzer6801
    @louisnemzer6801 Před rokem +1

    My favorite organic chemistry purification method!

  • @Dylan-cv7kj
    @Dylan-cv7kj Před rokem +28

    Science is so cool

  • @martinarenzi4744
    @martinarenzi4744 Před rokem +2

    Thank you Prof Dave! As always so precise and clear

  • @MSA_fansite
    @MSA_fansite Před rokem +1

    I love you mr.dave you are really helping beyond imagination

  • @prixynealojado6998
    @prixynealojado6998 Před 9 měsíci

    You're my hero, Professor Dave 🫶

  • @vspqrv9784
    @vspqrv9784 Před 4 měsíci

    such a high quality video and explanation

  • @nicco-sixty
    @nicco-sixty Před rokem +7

    Will you do more in-depth concepts in multivariable calculus, like the Jacobian matrix?

  • @similosihlegqalisisa8211

    I'm subscribing now Prof❤❤❤

  • @StephOnyia
    @StephOnyia Před 10 měsíci

    You are a pro 😮 Including the guy in the laboratory 😊

  • @TomasElizabeth
    @TomasElizabeth Před 3 měsíci

    So super cool

  • @milviodeleon4421
    @milviodeleon4421 Před rokem

    Wow comments on. Good job 👍

  • @missionsuccess6323
    @missionsuccess6323 Před 11 měsíci

    . Synthesis of 2-Amino-4-(substituted-phenyl)-1, 3-thi-
    azole Derivatives

  • @ansammkh1681
    @ansammkh1681 Před rokem

    thank you

  • @I_only_think_of_me
    @I_only_think_of_me Před rokem

    Fascinating

  • @rozana4470
    @rozana4470 Před rokem +1

    When are the other videos coming cause i start OC lab this week😭

  • @gamingwithrksaver4868

    We used to do these for derivative tests... and then match the m.p. to literature value to confirm the compound

  • @rassimsimou1594
    @rassimsimou1594 Před rokem +1

    Good

  • @RevilHermes
    @RevilHermes Před rokem +1

    I remember doing much simpler version with salt.

  • @enzoshii
    @enzoshii Před 9 měsíci

    Crystals did not form in our experiment. What could have gone wrong?

  • @WanderTheNomad
    @WanderTheNomad Před rokem +1

    5:17 Why do we have to use the minimum amount of solvent? Is it just to avoid wasting it or something? Or is there another reason?

    • @keypo790
      @keypo790 Před rokem

      Its because the experiments relies on Solubility Curve.

    • @user-qe8gy1zv2i
      @user-qe8gy1zv2i Před 11 měsíci

      its better to use the smallest amount of solvent to minimize the amount of material lost by retintion in the mother liqour

  • @krabre1848
    @krabre1848 Před rokem +2

    hi

  • @TheCosmicGuy0111
    @TheCosmicGuy0111 Před rokem

    Wowza

  • @judeboys6409
    @judeboys6409 Před rokem +3

    This video reminds me of being a meth head in my 20s. Wouldn’t recommend it 😂. I used to “wash” it in acetone. To clean out impurities .. Have no clue what that was doing scientifically. But it sure made you higher 😅😮. Hey Dave. What would be the science of that lol ? You probably more an idea than I

  • @harrybrielmann189
    @harrybrielmann189 Před rokem +1

    it's ok if the impurity is insoluble, just filter it out while hot.

  • @chrisaltaawesome
    @chrisaltaawesome Před rokem

    thank youuu

  • @tiptop1681
    @tiptop1681 Před 5 měsíci

    Finally i can do this with my meth. Thanks

  • @Linda-hn3bh
    @Linda-hn3bh Před rokem

    👍😌

  • @worldsfinestsimp6421
    @worldsfinestsimp6421 Před rokem

    TIGHT TIGHT TIGHT

  • @-JA-
    @-JA- Před rokem

    🙂👍

  • @livingcodex9878
    @livingcodex9878 Před rokem

    おはようございます

  • @desmond3828
    @desmond3828 Před rokem

    immunology?!

  • @krabre1848
    @krabre1848 Před rokem +1

    idk whats happening but cool

  • @kevinxavier2986
    @kevinxavier2986 Před rokem

    Komenke41

  • @KasaJiso
    @KasaJiso Před rokem

    First comment, day to of “do more flat earth vids they blew up.”
    Sorry not first I was too long to write the comment :(

    • @Gxlto
      @Gxlto Před rokem +3

      Sorry man I dont think he will. It's kind of dead at this point. I hope he does more creationism debunking

  • @DavidP089
    @DavidP089 Před rokem

    2 million subs and your videos barely reach 10k views 🤔🤔🤔

  • @white_isnt_a_race2338
    @white_isnt_a_race2338 Před rokem +1

    Educate me daddy