Chemistry 4all
Chemistry 4all
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Video

How to make a High Resolution Spectrometer
zhlédnutí 38KPřed 5 lety
Today, we will be making a DIY high resolution spectrometer. The pdf file can be downloaded here: publiclab.org/notes/homechemist/08-24-2018/diy-high-resolution-spectrometer
How to make ethyl acetate| Part 2 (Fractional distillation)
zhlédnutí 4,4KPřed 5 lety
In this video, we will see how to purify the crude ethyl acetate obtained in a previous video by means of fractional distillation.
How to make ethyl acetate | Part 1 (Synthesis + Raman analysis)
zhlédnutí 10KPřed 5 lety
Today, we will be making some ethyl acetate by means of a classic esterification reaction.The final product turned out to be contaminated with significant amounts of ethanol, and so we will try to purify the product obtained in a future video. Additional notes: -The raman spectra were taken with a professional 785 nm raman equipment, since the power supply of my DIY raman spectrometer is not wo...
How to work under inert atmosphere/Making anhydrous ethanol
zhlédnutí 4,1KPřed 6 lety
This video shows how to make anhydrous ethanol starting from regular 96% ethanol , besides that the video shows how to work under Argon atmosphere
How to make methyl benzoate
zhlédnutí 7KPřed 6 lety
This video shows how to make methyl benzoate starting from benzoic acid (that we have previously made in another video) by terms of a classical fischer esterification reaction.
How to make Benzoic acid from Toluene
zhlédnutí 27KPřed 6 lety
The video shows how to make pure benzoic acid out from toluene by terms of a classical oxidation of the benzylic position of the aryl derivative
How to make toluene
zhlédnutí 21KPřed 6 lety
The video shows how to make pure toluene out from a toluene based paint remover by terms of a fractional distillation
Homemade Raman Spectroscopy
zhlédnutí 50KPřed 6 lety
This video shows how to make and operate a homemade raman spectrometer
How to extract geraniol from an insect repellent
zhlédnutí 3KPřed 6 lety
The video shows how to isolate pure geraniol out from a plant based insect repellent
How to make oil of wintergreen
zhlédnutí 6KPřed 6 lety
This video shows how to make oil of wintergreen starting from salicylic acid
How to make salicylic acid
zhlédnutí 13KPřed 7 lety
How to make salicylic acid
How to purify Aspirin?
zhlédnutí 5KPřed 7 lety
How to purify Aspirin?
How to extract Aspirin
zhlédnutí 5KPřed 7 lety
How to extract Aspirin
Extracción de Aspirina
zhlédnutí 38KPřed 7 lety
Este vídeo muestra la extracción de la aspirina a partir de aspirina comercial
Redox chemistry
zhlédnutí 143Před 7 lety
Redox chemistry
The Clock Reaction
zhlédnutí 649Před 7 lety
The Clock Reaction
How to extract cinnamaldehyde from cinnamon bark
zhlédnutí 12KPřed 7 lety
How to extract cinnamaldehyde from cinnamon bark
How to make a silver mirror
zhlédnutí 3,5KPřed 7 lety
How to make a silver mirror
How to extract vanillin
zhlédnutí 8KPřed 7 lety
How to extract vanillin
Soxhlet Extraction of Curcumin from Turmeric
zhlédnutí 62KPřed 7 lety
Soxhlet Extraction of Curcumin from Turmeric
Column chromatography
zhlédnutí 1,3KPřed 7 lety
Column chromatography
How to make Hot Ice
zhlédnutí 478Před 7 lety
How to make Hot Ice
Sodium Acetate(Hot Ice) Synthesis
zhlédnutí 3,7KPřed 7 lety
Sodium Acetate(Hot Ice) Synthesis
Isolation of limonene
zhlédnutí 1,6KPřed 7 lety
Isolation of limonene
Reacción ácido sulfúrico y azúcar/dehydratation of sugar by sulfuric acid
zhlédnutí 387Před 8 lety
Reacción ácido sulfúrico y azúcar/dehydratation of sugar by sulfuric acid

Komentáře

  • @heuerde6582
    @heuerde6582 Před 2 měsíci

  • @NegarAzar-xi1mw
    @NegarAzar-xi1mw Před 2 měsíci

    Hi Thank you for your video I have a question what is the temperature for the first step?

  • @abdulmobeenshaikh9593
    @abdulmobeenshaikh9593 Před 5 měsíci

    I am supply high curcumin turmeric mother

  • @victoribarra9930
    @victoribarra9930 Před 6 měsíci

    Great job !

  • @williambradley611
    @williambradley611 Před 6 měsíci

    Toluene has not been proven to be carcinogenic but has been proved to be toxic and can cause birth defects.

  • @SciDOCMBC
    @SciDOCMBC Před 7 měsíci

    Why are you putting two cannulas in the rubber septum? The Erlenmayer flask (which is actually not suitable for vacuum) has already been evacuated, so its a vacuum inside the flask. If you now attach a balloon filled with argon, the argon fills the entire wrong one (VACCUM!). There is no need for flushing.

  • @NoahKainWhittington
    @NoahKainWhittington Před 7 měsíci

    your lasers look like 12v lasers. They will run on 3 volts?

  • @rusticagenerica
    @rusticagenerica Před 8 měsíci

    Would it work if you used a BluRay?

  • @alessandromarini-kt6ur

    Hi I would like to know how Is powered the Science-Surplus spectrometer becaude I lose the 5 V Power supply and i don't want to male any mistakes. Thank you

  • @robertoroeder2716
    @robertoroeder2716 Před rokem

    Voy a hacerlo a ver si funciona como insecticida, gracias!

  • @farzadjani3592
    @farzadjani3592 Před rokem

    Thanks for sharing the video. I am interested in experimenting with a CCTV camera that has a varifocal lens instead of a Canon camera. Could you please tell me the magnification level (X) of the Canon camera you used, taking into consideration the distance from the camera to the diffraction grating?

  • @currutaca1981
    @currutaca1981 Před rokem

    could you make a video explaining How to process the data obtained by a spectrometer

  • @double0prime
    @double0prime Před rokem

    What angle should the rays hit the dvd at? And did you need to split the dvd layers to isolate the gradient? Many thanks!

  • @Refertech101
    @Refertech101 Před rokem

    Sodium acetate can be purified further by dissolving in Dry methanol, non saturated solution, hot filter out the solid impurities, boil down, then chill the alcohol in the freezer and filter out the pure crystals. Methanol vapours are hazardous if in a non vented room, So if you are more advanced in skill Simply ensure good ventilation or done out side, being an alcohol it is flammable. I use it to make Glacial Acetic acid, and Acetic Anhydride via Sulphur Bromide method

  • @zodd0001
    @zodd0001 Před rokem

    I am a chemist and make videos about, do you want to exchange subscriptions ? I performed a pilot scale pyrolysis of waste water bottles: czcams.com/video/VrfCl6Fnwo0/video.html

  • @kallah4999
    @kallah4999 Před rokem

    You distilled toluene, you didn`t make it. Maybe just change the discription. I usually wash it to get out most of the more water soluble, fractionate it, then remove water with a Dean Stark trap. Do a nitro reduction with sodium dithionite whit ratios. Don`t think it`s been done other then by Chemplayer in a series of micro scale reduction trails where dithionite came out as clearly best with a 30 min reflux and no steam distillation of end product, only vacuum filtration. I think he could have done a better work up, but it wasn`t really the meaning of the video. Simple distillation and drying with CaCl2 would probably have done much.

  • @iq18oo30
    @iq18oo30 Před rokem

    You should teach you how to make sodium hypophosphorus. I'm going to use it to make hypophosphorous acid.

  • @cyberspider78910
    @cyberspider78910 Před rokem

    43% only.!!

  • @geopolitikNEWSLCT
    @geopolitikNEWSLCT Před 2 lety

    Se puede hacer no co acetona sino con otro disolvente?

  • @EarlWallaceNYC
    @EarlWallaceNYC Před 2 lety

    Isn't the DVD closer than the minimum FL of the lens (0.38 m aka14.96″)? Doesn't this cause blurriness? Great video. Thanks for sharing.

  • @Aragmatiki
    @Aragmatiki Před 2 lety

    I want to make one too for my homelab. What's the budget?

  • @Roel922
    @Roel922 Před 2 lety

    Very interesting presentation. Only thing is it's hard listenand follow what's being said because the recording sound is to low.

  • @thatdiyguyraymondmonk1225

    Thanks. Good information but; I really dislike computer voice.

  • @mlwasubramanian4905
    @mlwasubramanian4905 Před 2 lety

    poor sound.

  • @MrMrannoying
    @MrMrannoying Před 2 lety

    Ah, so in this extraction you just have to get the water boiling, not exactly the cinnamaldehyde itself to boil? I was looking at the boiling point of cinnamaldehyde and was like oh man that is HIGH! But I guess from this video, the water can trap the small amount of cinnamaldehyde vapor above the liquid and carry it over?

  • @ericopera
    @ericopera Před 2 lety

    Wich is the yield?

  • @sanandsahoo2579
    @sanandsahoo2579 Před 2 lety

    Nyc arrangement and whats its cost ?

  • @CloudScience
    @CloudScience Před 2 lety

    Owsome experiment

  • @rajarestorasi2tak247
    @rajarestorasi2tak247 Před 2 lety

    Mixing ratio poeder hydroxyde ????

  • @juliaalmaraz7355
    @juliaalmaraz7355 Před 2 lety

    Muy buen video. Química.arg. Lidocaína en polvo. BenzoCaína, Mepivacaina. Cafeína blanca. Etc Productos odontología. Venta importador directo. Servicios químicos. Dra. Julia Alma. +54 3492 275121 JuliaAlmaraz55@gmail.com

  • @mikegLXIVMM
    @mikegLXIVMM Před 2 lety

    This is one of the Top Raman spectrometers in the country!

  • @CamilaMile
    @CamilaMile Před 2 lety

    Saben cuánto tiempo toma en cristalizarse el ácido acetilsalicílico?

  • @user-tc3hv8pb9d
    @user-tc3hv8pb9d Před 2 lety

    I need a method for preparing ethyl acetate from acetaldehyde, how do I get it?

  • @hurdleyrowe891
    @hurdleyrowe891 Před 3 lety

    Where did you get equipment from

  • @mssagar1892
    @mssagar1892 Před 3 lety

    Thank you 😌🙏

  • @shades5457
    @shades5457 Před 3 lety

    Thank you for this very informative video. It really helped me in my studies. May I ask how did you determine the density which is implied to be 0.84 g/ml?

  • @ExemplaryLigas
    @ExemplaryLigas Před 3 lety

    Eres de México?

  • @somi6323
    @somi6323 Před 3 lety

    Software name pls?

  • @blacktellez4108
    @blacktellez4108 Před 3 lety

    En Resumen Coca....INA artesanal🤔🤔🤔

  • @naasikhendricks1501
    @naasikhendricks1501 Před 3 lety

    Where did you source filters

  • @daithiod
    @daithiod Před 3 lety

    Superb work. I wonder if I could use it at my high school here in Japan as an extracurricular project. I miss the joy of doing science!!

  • @aarondrake6409
    @aarondrake6409 Před 3 lety

    I am going to try this one - Thanks!

  • @syifasalsabila9885
    @syifasalsabila9885 Před 3 lety

    🥲

  • @illya.ruslanovichshevchenk4106

    Acetic acid is HOAc, not HAc

  • @skyrim4622
    @skyrim4622 Před 3 lety

    world best cinnamon (Ceylon cinnamon) available. please contact me...!!!! shehankaushalye@gmail.com

  • @kkevan4138
    @kkevan4138 Před 3 lety

    Thank you very much for this, it was easy and clear to follow! Keep it up :D

  • @waelkhalil95
    @waelkhalil95 Před 3 lety

    How to do fractination to the product mixture??

  • @gracianolopez3053
    @gracianolopez3053 Před 3 lety

    No entiendo, extraer aspirina de aspirina? Cual es la razón o ventaja, estoy confundido

    • @adriintheriver7435
      @adriintheriver7435 Před 3 lety

      la pastilla de aspirina contiene muchas mas cosas aparte del medicamento en si, es decir, lo que se hace en el video es quitar todos los otros compuestos que tienen las pastillas y quedarse solo con el ácido acetilsalicílico, que es el medicamento que tienen las aspirinas.

    • @user-qc5ms3mc4f
      @user-qc5ms3mc4f Před 2 lety

      @@adriintheriver7435 A eso se le llama extraccion en quimica orgánica, en este caso "purifica" la aspirina. Aisló el componente activo de los incipientes.

  • @insanitywolf05
    @insanitywolf05 Před 3 lety

    Really cool! Thanks for sharing your setup. Obtaining those raman filters is a pain an therefore I wonder whether you could just attach a self-built linear ccd-based spectrometer and cover the spectrsl line where the laser wavelength is projected on the ccd with a delicate line of really black paint (black 3.0). Can't you get around the need for an unaffordable notch or edge filter this way?

  • @stevelibby3
    @stevelibby3 Před 3 lety

    Have you considered using vacuum to lower boiling temperatures?