Webinar recording: Karl Fischer titration - Troubleshooting, tips and tricks

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  • čas přidán 8. 06. 2021
  • Watch this recorded webinar to learn how to avoid or fix commonly encountered problems in water content determination with Karl Fischer titration, particularly relating to:
    - the coulometric or volumetric titration cell,
    - conditioning before titration,
    - the Karl Fischer electrodes (maintenance, storage, and cleaning),
    - titer determination,
    - sample addition and sample preparation,
    - and more.
    For more information, check out our Product Help Center
    www.metrohm.com/en/service/pr...
  • Věda a technologie

Komentáře • 16

  • @rahnpincas142
    @rahnpincas142 Před 4 dny

    Hi, our mining lab has just purchased an Eco Titrator 10080010 to be used for copper analysis via iodimetry. Can someone share a reference on how to set up the method using Eco Titrator? we have been using manual buret for iodometry, so this one is basically an upgrade. Thank you!

  • @LilGugz
    @LilGugz Před 2 lety

    That first question... no - you can't clean an electrode in the dishwasher... WOW! Would love to see actual demonstrations with the Metrohm instruments of calibrations, equipment, issues, etc. Thanks for the presentation :-)

    • @MetrohmTV
      @MetrohmTV  Před 2 lety +1

      Hi
      You're welcome! If you're interested in electrode handling, you can find videos on this on our website:
      www.metrohm.com/en/support-and-service/electrode-maintenance/
      And if you're interested in longer presentations, you can find more in our Webinar Center:
      www.metrohm.com/en/support-and-service/webinar-center/

  • @pastelpinks
    @pastelpinks Před 9 měsíci

    Hi what if there is backflow of cell solution back into the titrant Comp T5 tube and instead of dosing titrant it is dosing the cell solution back into the cell

    • @MetrohmTV
      @MetrohmTV  Před 9 měsíci

      Hi
      We cannot tell what the problem might be without further information. Please contact your local Metrohm subsidiary or exclusive distributor for technical support in this matter:
      www.metrohm.com/en.html#country-selection
      Best regards
      Michel, Metrohm International Headquarters

  • @hafiyarahmania5013
    @hafiyarahmania5013 Před rokem

    What causes the machine keep shutting down and starting back up (restarting) in the middle of titration?thanks

    • @MetrohmTV
      @MetrohmTV  Před rokem +1

      Hi Hafiya
      This should not happen. Please contact your local Metrohm organization or exclusive distributor for technical support. They will be able to help you out. You can find the contact details on our website: www.metrohm.com/
      Best regards
      Metrohm International Headquarters

  • @mharuphaadebukola6812
    @mharuphaadebukola6812 Před 2 lety

    What if you're trying to empty the content of the titration vessel and it's not moving from the vessel to the waste bottle
    What could probably cause that?

    • @MetrohmTV
      @MetrohmTV  Před 2 lety

      Hi
      The most probable cause is a leak between titration vessel and waste bottle. Check all tubing connections and also check the cap on the waste bottle.
      If this doesn't help, please get in touch with your local Metrohm service engineer.
      Best regards
      Metrohm International Headquarters

  • @mostafaosama6691
    @mostafaosama6691 Před rokem

    Hi sir
    The methanol fill the cup without stop how to fix it ?

    • @MetrohmTV
      @MetrohmTV  Před rokem

      Hi Mostafa
      Thank you for your comment. The best way to get technical support is to contact your local Metrohm subsidiary or exclusive distributor. You can find the contact details on our website:
      www.metrohm.com/en.html#country-selection
      Best regards
      Michel, Metrohm International Headquarters

  • @ramamohankilli5548
    @ramamohankilli5548 Před 4 měsíci

    On what cases Water content result came zero, but the regular sample trend is 15%

    • @MetrohmTV
      @MetrohmTV  Před 4 měsíci

      Hi
      Thank you for your comment. This problem could be due to a variety of reasons. Therefore, to get to the bottom of this, we recommend that you contact your local Metrohm organization or exclusive distributor.
      BR
      Michel, Metrohm International Headquarters

  • @sachingaikar1197
    @sachingaikar1197 Před rokem

    Sir, starrier not start

    • @MetrohmTV
      @MetrohmTV  Před rokem

      Hi Sachin
      Please contact your local Metrohm subsidiary or exclusive distributor for technical support. You can find the contact details on our website: www.metrohm.com
      BR
      Metrohm International Headquarters

    • @sachingaikar1197
      @sachingaikar1197 Před rokem

      @@MetrohmTV thanks sir