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Pressurized sample infusion
How to set up a PSI flask to monitor a chemical reaction using ESI-MS
See doi.org/10.1002/cmtd.202100068 for more details
zhlédnutí: 236

Video

Glovebox operationGlovebox operation
Glovebox operation
zhlédnutí 209Před měsícem
Using the MBraun Labmaster: transferring chemicals and equipment in and out of the box
Testing solvents for peroxideTesting solvents for peroxide
Testing solvents for peroxide
zhlédnutí 481Před 9 měsíci
How to test solvents for the presence of peroxides using simple peroxide test strips
How to change the capillary on an electrospray ionization mass spectrometerHow to change the capillary on an electrospray ionization mass spectrometer
How to change the capillary on an electrospray ionization mass spectrometer
zhlédnutí 560Před rokem
Specifically, the Waters TQD ("Triple Quad Detector") instrument.
Fume Hood SafetyFume Hood Safety
Fume Hood Safety
zhlédnutí 354Před rokem
Safe use of fume hoods. For more information, consult www.uvic.ca/ohse/research/laboratory/fumehoods/index.php
DataGrab Python script tutorialDataGrab Python script tutorial
DataGrab Python script tutorial
zhlédnutí 112Před rokem
How to use the script for extracting MassLynx data. Code available at GitHub.com/Chagunda/DataGrab
UVic Chem101 BalancesUVic Chem101 Balances
UVic Chem101 Balances
zhlédnutí 343Před 2 lety
How to use a balance in the UVic Chem101 Laboratory. See web.uvic.ca/~mcindoe/101/balance.gif for a quick summary gif
UVic Chem101 SpectrometerUVic Chem101 Spectrometer
UVic Chem101 Spectrometer
zhlédnutí 256Před 2 lety
How to use a pipette in the UVic Chem101 Laboratory. See web.uvic.ca/~mcindoe/101/spec.gif for a quick summary gif
UVic Chem101 TitrationUVic Chem101 Titration
UVic Chem101 Titration
zhlédnutí 392Před 2 lety
How to use a pipette in the UVic Chem101 Laboratory. See web.uvic.ca/~mcindoe/101/titration.gif for a quick summary gif
UVic Chem101 Vacuum FiltrationUVic Chem101 Vacuum Filtration
UVic Chem101 Vacuum Filtration
zhlédnutí 336Před 2 lety
How to perform a vacuum filtration in the UVic Chem101 Laboratory. See web.uvic.ca/~mcindoe/101/vacfilt.gif for a quick summary gif
UVic Chem101 PipettingUVic Chem101 Pipetting
UVic Chem101 Pipetting
zhlédnutí 94Před 2 lety
How to use a pipette in the UVic Chem101 Laboratory. See web.uvic.ca/~mcindoe/101/pipette.gif for a quick summary gif
Needle handling in the chemistry laboratoryNeedle handling in the chemistry laboratory
Needle handling in the chemistry laboratory
zhlédnutí 2,2KPřed 2 lety
How to handle needles safely. See the article "Safe Handling of Cannulas and Needles in Chemistry Laboratories" by Chandra, Zebrowski and Lenertz (pubs.acs.org/doi/10.1021/acs.chas.1c00069) for more details
Cannula transferCannula transfer
Cannula transfer
zhlédnutí 3,4KPřed 2 lety
How to perform a cannula transfer, including adjusting the flow rates and cleaning the double-ended stainless-steel needle afterwards.
Lab Procedures in Case of FireLab Procedures in Case of Fire
Lab Procedures in Case of Fire
zhlédnutí 444Před 2 lety
Fire hazards, fire extinguisher and pull station locations, evacuation plan, exits, procedures, safe departure, annunciator. Presented specifically for the McIndoe Lab at UVic, BC, Canada.
How to perform a vacuum sublimationHow to perform a vacuum sublimation
How to perform a vacuum sublimation
zhlédnutí 14KPřed 4 lety
How to purify a volatile organic compound via sublimation. Great for getting nice white crystals from yellow goo!

Komentáře

  • @leyla6872
    @leyla6872 Před 4 dny

    really needed this tutorial! Thanks for sharing!

  • @thesentientneuron6550

    Hi there! Thank you so much for sharing this interesting analysis technique! I’d heard about how argon gas flow can carry reactants outside the reaction chamber and find it really interesting that you use this property to carry out real-time reaction monitoring. Are there any limitations on the kinds of reactions that can be done with this technique? What about reactions that happen largely in the solid state (like the synthesis of YBCO or thermite, for example?)

  • @acmhfmggru
    @acmhfmggru Před 27 dny

    why are you bothering with a lab coat if you aren't going to wear it properly? this isn't a fashion show... get rid of the jewellery and do up your jacket, you are meant to be a model for the students, so act like it.

    • @thesentientneuron6550
      @thesentientneuron6550 Před 26 dny

      I’m reporting you for harassment. Who are you to judge whether or not she wears jewellery? She has no obligation to fit your perception of a model student, and she is following all proper lab safety protocols befitting her station. If you have nothing better to do besides berate someone who is sharing genuinely interesting information while not discussing the actual topic being presented in the video, I suggest you go outside and touch some grass. And don’t bother trying to get a reply or response from me. I don’t care about what you have to say about me.

    • @acmhfmggru
      @acmhfmggru Před 26 dny

      @@thesentientneuron6550 because it is dangerous. because of fires and splashes. grow up, safety is job number 1.

  • @Acceleratedpayloads
    @Acceleratedpayloads Před 29 dny

    I thought your shirt was a hospital gown lol

  • @KatKrouse
    @KatKrouse Před měsícem

    What type of plug into the wall do you need for this system's power?

  • @eas605
    @eas605 Před 3 měsíci

    Which Temperatur are you using for the Regeneration

  • @user-yr2nb4vr3q
    @user-yr2nb4vr3q Před 4 měsíci

    My mother has this birthmark on her leg and in the 70s a GP put liquid nitrogen on it claiming it will remove it 🤮

  • @drabsiddique
    @drabsiddique Před 4 měsíci

    Dont we need to work on the control panel before and after the changing?

  • @rismaldavieri
    @rismaldavieri Před 4 měsíci

    very helpfull, thank you for the explanation

  • @zacklantz8181
    @zacklantz8181 Před 5 měsíci

    I have a used older lct ms, curious if you wouldn't mind sharing some pc connection info. I have the pc, optical card, and is recognized but I'm not sure if I have everything that is required to connect to the tcd card. Many thanks!

  • @Fandikusnadi1979
    @Fandikusnadi1979 Před 8 měsíci

    On meniute 4 30 what liquid it pour to container?

  • @user-bn7sn3du4g
    @user-bn7sn3du4g Před 8 měsíci

    Thank you very much !! This video saved two students..

  • @user-ds9pt2wx1i
    @user-ds9pt2wx1i Před 8 měsíci

    Thank you sir ....this video more more usefull me sir thank you for thos usefull video

  • @rentaros6475
    @rentaros6475 Před 9 měsíci

    Always, ALWAYS let the pump run for a few minutes and turning on the vacuum BEFORE you cool the solvent trap. You can get liquid oxygen in it if you do it this way.

  • @gnarstypow
    @gnarstypow Před 9 měsíci

    I would really recommend just disconnecting the keg and refilling it in the fume hood. You're definitely inhaling a lot of solvent vapors while pouring in the open lab. Then you can degas in the hood without running a tripwire across the aisle.

  • @mnemonicallysathyan4339
    @mnemonicallysathyan4339 Před 10 měsíci

    THANK YOU

  • @josephdahdouh2725
    @josephdahdouh2725 Před 11 měsíci

    So, is the pure product going from solid to gas. And then the adaptor like object that is inserted, its job is to crystallize the sublimated pure product? Is that how you separate 2solids from each other. How do you even know that the other solid won't also be binding to the glass thingy that you scraped of the product at the end too. Via NMR?

    • @mcindoegroup
      @mcindoegroup Před 11 měsíci

      Yes, you are subliming a volatile product away from involatile impurities. The cold finger collects the product. Purity can be checked by any method you'd normally use, NMR included

  • @MichaelLapore-lk9jz

    Could you also put argon into the system?

  • @user-ru8qw8sh7p
    @user-ru8qw8sh7p Před rokem

    Really thank you 👍

  • @saeedhashemi4762
    @saeedhashemi4762 Před rokem

    Really thank you 👍

  • @jeffaguinaga1447
    @jeffaguinaga1447 Před rokem

    Thank you for the instruction

  • @GnosisMan50
    @GnosisMan50 Před rokem

    THANK YOU!! Just what I needed to know.

  • @momsmushroomsjodyfoster5786

    I was a scientist in my first life😂

  • @momsmushroomsjodyfoster5786

    I think smart people are very attractive 😊

  • @boilshifter1350
    @boilshifter1350 Před rokem

    I'm not in yet 10sen. and the only thing I can think of is how incredibly cute you look

  • @Xaddre
    @Xaddre Před rokem

    I didnt know Kwebbelkop was a scientist

  • @Transiltommus
    @Transiltommus Před rokem

    good video, maybe get a better microphone :)

  • @pramodhsrihari493
    @pramodhsrihari493 Před rokem

    Won't inserting and removing the needles from the rubber covers of the flask cause oxygen from the atmosphere to enter the flask?

    • @raghuvenkatesan6792
      @raghuvenkatesan6792 Před 11 měsíci

      if it is already filled with argon, the argon is more dense than air so air cannot get in

  • @jesscorbin5981
    @jesscorbin5981 Před rokem

    What is the black residue exactly?

  • @leeknoz935
    @leeknoz935 Před rokem

    I didn't learn anything only have more question

  • @baldskier5530
    @baldskier5530 Před rokem

    And don't drop the tiny bar down the drain. 😫

  • @JeremyKaplitt
    @JeremyKaplitt Před rokem

    Very helpful, thank you!

  • @georgebernacchi1532

    Too dangerous the way she does this. Nitrogen??? Why. Chiller or ice water.

  • @SeriousPigi
    @SeriousPigi Před rokem

    "this video is not a substitute for proper lab training", meanwhile in many labs they just say go and figure it out

  • @dr.dineshsawant8872

    Better to use magnetic stirrer and stirring bar for proper mixing of nitrogen and fast degasing

  • @chrisjefford5896
    @chrisjefford5896 Před 2 lety

    💖 𝕡𝐫o𝕄o𝔰𝓶

  • @koumyayassine1558
    @koumyayassine1558 Před 2 lety

    Thank you

  • @thecros1076
    @thecros1076 Před 2 lety

    Can I adjust the pressure to 50 bars on output side ?

  • @gauravjyotid.kalita3417

    Thanks a lot for the information.

  • @Joe_Yacketori
    @Joe_Yacketori Před 2 lety

    Wait... why were some of those stir bars so dark? They're coated in PTFE, right? Shouldn't PTFE resist all chemical attack except that of a short list of exotic chemicals?

    • @mcindoegroup
      @mcindoegroup Před 2 lety

      mostly an accumulation of insoluble colored compounds in micro abrasions on the bars

  • @minusstage3
    @minusstage3 Před 2 lety

    Love those canisters!

  • @HuniHunji
    @HuniHunji Před 2 lety

    Thank you! This video helps me so much!

  • @mr.chindo8570
    @mr.chindo8570 Před 2 lety

    999th subscriber

  • @Sp-fe1eo
    @Sp-fe1eo Před 2 lety

    thanks for the video...it's really helpful and give me more knowledge about rotovap

  • @sorkeror
    @sorkeror Před 2 lety

    Cool, I've never heard about vacuum destillation before I saw a bottle of whisky from a Swedish distillery where they actually use it

  • @learningtolivewithhumans1859

    most informative one i could find thanks bro

  • @kpedretty3012
    @kpedretty3012 Před 2 lety

    We told you multiple times... stop using the MS vial dish for water baths

  • @emreakbulut5378
    @emreakbulut5378 Před 2 lety

    vaaooovvv ommmggggg

  • @pharmasolutionpakistan7668

    Good

  • @pharmasolutionpakistan7668

    Good